1. Scope

1.1 This test method establishes a procedure to measure the susceptibility of steel to a time-delayed failure such as that caused by hydrogen. It does so by measuring the threshold for the onset of subcritical crack growth using standard fracture mechanics specimens, irregular-shaped specimens such as notched round bars, or actual product such as fasteners (2) (threaded or unthreaded) springs or components as identified in SAE J78, J81, and J1237.

1.2 This test method is used to evaluate quantitatively:

1.2.1 The relative susceptibility of steels of different composition or a steel with different heat treatments;

1.2.2 The effect of residual hydrogen in the steel as a result of processing, such as melting, thermal mechanical working, surface treatments, coatings, and electroplating;

1.2.3 The effect of hydrogen introduced into the steel caused by external environmental sources of hydrogen, such as fluids and cleaners maintenance chemicals, petrochemical products, and galvanic coupling in an aqueous environment.

1.3 The test is performed either in air, to measure the effect if residual hydrogen is in the steel because of the processing (IHE), or in a controlled environment, to measure the effect of hydrogen introduced into the steel as a result of the external sources of hydrogen (EHE) as detailed in ASTM STP 453.

1.4 The values stated in acceptable U.S. units shall be regarded as the standard. The values stated in metric units may not be exact equivalents. Conversion of the U.S. units by appropriate conversion factors is required to obtain exact equivalence.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use .

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

A490 Specification for Structural Bolts, Alloy Steel, Heat Treated, 150 ksi Minimum Tensile Strength

A574 Specification for Alloy Steel Socket-Head Cap Screws

B602 Test Method for Attribute Sampling of Metallic and Inorganic Coatings

E4 Practices for Force Verification of Testing Machines

E6 Terminology Relating to Methods of Mechanical Testing

E8 Test Methods for Tension Testing of Metallic Materials

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E399 Test Method for Linear-Elastic Plane-Strain Fracture Toughness K Ic of Metallic Materials

E812 Test Method for Crack Strength of Slow-Bend Precracked Charpy Specimens of High-Strength Metallic Materials

E1681 Test Method for Determining Threshold Stress Intensity Factor for Environment-Assisted Cracking of Metallic Materials

F519 Test Method for Mechanical Hydrogen Embrittlement Evaluation of Plating/Coating Processes and Service Environments

F606 Test Methods for Determining the Mechanical Properties of Externally and Internally Threaded Fasteners, Washers, Direct Tension Indicators, and Rivets

F2078 Terminology Relating to Hydrogen Embrittlement Testing

G5 Reference Test Method for Making Potentiostatic and Potentiodynamic Anodic Polarization Measurements

G129 Practice for Slow Strain Rate Testing to Evaluate the Susceptibility of Metallic Materials to Environmentally Assisted Cracking

SAE Standards

ANSI/ASME

Keywords

decreasing loading rate; delayed brittle failure; displacement control; fasteners; hydrogen embrittlement threshold; hydrogen induced stress cracking; rising step load; slow strain rate;

ICS Code

ICS Number Code 77.040.10 (Mechanical testing of metals)

DOI: 10.1520/F1624-00

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