1. Scope

1.1 This test method covers the procedure for determining the shear and bending fatigue performance of calcium phosphate coatings and of porous and nonporous metallic coatings and for determining the bending fatigue performance of metallic coatings oversprayed with calcium phosphate. This test method has been established based on plasma-sprayed titanium and plasma-sprayed hydroxylapatite coatings. The efficacy of this test method for other coatings has not been established. In the shear fatigue mode this test method evaluates the adhesive and cohesive properties of the coating on a metallic substrate. In the bending fatigue mode this test method evaluates both the adhesion of the coating as well as the effects that the coating may have on the substrate material. These methods are limited to testing in air at ambient temperature. These test methods are not intended for application in fatigue tests of components or devices; however, the test method which most closely replicates the actual loading configuration is preferred.

1.2 The values stated in SI units are to be regarded as the standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

E6 Terminology Relating to Methods of Mechanical Testing

E206 Definitions of Terms Relating to Fatigue Testing and the Statistical Analysis of Fatigue Data; Replaced by E 1150

E466 Practice for Conducting Force Controlled Constant Amplitude Axial Fatigue Tests of Metallic Materials

E467 Practice for Verification of Constant Amplitude Dynamic Forces in an Axial Fatigue Testing System

E468 Practice for Presentation of Constant Amplitude Fatigue Test Results for Metallic Materials

E1012 Practice for Verification of Testing Frame and Specimen Alignment Under Tensile and Compressive Axial Force Application

Keywords

ceramic coatings; composite coatings; fatigue testing; hydroxylapatite; metallic coatings; plasma-sprayed coatings; porous coatings; tribasic calcium phosphate; Bend testing--surgical materials; Bonding; Coatings (surgical implants); Constant-load-amplitude fatigue crack growth rates; Fatigue--surgical implant materials; Loading tests--surgical materials/applications; Metallic coatings; Performance--medical materials/applications; Porosity--medical/surgical materials; Shear testing--medical materials/applications; Stress; Surface analysis

ICS Code

ICS Number Code 25.220.40 (Metallic coatings)

DOI: 10.1520/F1160-00E01

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