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  • ASTM
    E793-06(2012) Standard Test Method for Enthalpies of Fusion and Crystallization by Differential Scanning Calorimetry
    Edition: 2012
    $91.10
    Unlimited Users per year

Description of ASTM-E793 2012

ASTM E793-06-Reapproved2012

Historical Standard: Standard Test Method for Enthalpies of Fusion and Crystallization by Differential Scanning Calorimetry




ASTM E793

Scope

1.1 This test method describes the determination of the enthalpy (heat) of fusion (melting) and crystallization by differential scanning calorimetry (DSC).

1.2 This test method is applicable to solid samples in granular form or in any fabricated shape from which an appropriate specimen can be cut, or to liquid samples that crystallize within the range of the instrument. Note, however, that the results may be affected by the form and mass of the specimen, as well as by other experimental conditions.

1.3 The normal operating temperature range is from −120 to 600°C. The temperature range can be extended depending upon the instrumentation used.

1.4 This test method is generally applicable to thermally stable materials with well defined endothermic or exothermic behavior.

1.5 Computer or electronic based instruments, techniques, or data treatment equivalent to those in this test method may also be used.

1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7 The enthalpy of melting and crystallization portion of ISO 11357-3 is equivalent to this standard.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


Keywords

crystallization; differential scanning calorimeter; DSC; energy; enthalpy; fusion; heat; melting


ICS Code

ICS Number Code 17.200.10 (Heat. Calorimetry)


DOI: 10.1520/E0793-06R12

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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