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  • ASTM
    E2465-13 Standard Test Method for Analysis of Ni-Base Alloys by Wavelength Dispersive X-Ray Fluorescence Spectrometry
    Edition: 2013
    $113.57
    Unlimited Users per year

Description of ASTM-E2465 2013

ASTM E2465 - 13

Standard Test Method for Analysis of Ni-Base Alloys by Wavelength Dispersive X-Ray Fluorescence Spectrometry

Active Standard ASTM E2465 | Developed by Subcommittee: E01.08

Book of Standards Volume: 03.05




ASTM E2465

Significance and Use

5.1 This procedure is suitable for manufacturing control and for verifying that the product meets specifications. It provides rapid, multi-element determinations with sufficient accuracy to assure product quality. The analytical performance data included may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy, or if the performance of a particular spectrometer has changed.

1. Scope

1.1 This test method covers the analysis of Ni-base alloys by wavelength dispersive X-ray Fluorescence Spectrometry for the determination of the following elements:

Element

Composition Range

Manganese

0.06?% to 1.6?%

Phosphorus

0.008?% to 0.015?%

Silicon

0.08 % to 0.6?%

Chromium

1.6?% to 22?%

Nickel

23?% to 77?%

Aluminum

0.20?% to 1.3?%

Molybdenum

0.03?% to 10?%

Copper

0.007?% to 2.5?%

Titanium

0.11?% to 3.0?%

Niobium

0.55?% to 5.3?%

Iron

0.17?% to 46?%

Tungsten

0.06?% to 0.50?%

Cobalt

0.04?% to 0.35?%


Note 1 Unless exceptions are noted, concentration ranges can be extended by the use of suitable reference materials. Once these element ranges are extended they must be verified by some experimental means. This could include but not limited to Gage Repeatability and Reproducibility studies and/or Inter-laboratory Round Robin studies. Once these studies are completed, they will satisfy the ISO 17025 requirements for capability.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

Other Documents

ISO 17025 General requirements for the competence of testing and calibration laboratories

ASTM Standards

E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials

E305 Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves

E1361 Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis

E1601 Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method

E1622 Practice for Correction of Spectral Line Overlap in Wavelength-Dispersive X-Ray Spectrometry


Keywords

Ni-base alloys; spectrometric analysis; X-ray emissions; X-ray fluorescence;


ICS Code

ICS Number Code 77.040.20 (Non-destructive testing of metals); 77.120.50 (Titanium and titanium alloys)


DOI: 10.1520/E2465

ASTM International is a member of CrossRef.

ASTM E2465

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