1. Scope

1.1 This test method covers the determination of a reference temperature, T _o , which characterizes the fracture toughness of ferritic steels that experience onset of cleavage cracking at elastic, or elastic-plastic K _Jc instabilities, or both. The specific types of ferritic steels (3.2.1) covered are those with yield strengths ranging from 275 to 825 MPa (40 to 120 ksi) and weld metals, after stress-relief annealing, that have 10 % or less strength mismatch relative to that of the base metal.

1.2 The specimens covered are fatigue precracked single-edge notched bend bars, SE(B), and standard or disk-shaped compact tension specimens, C(T) or DC(T). A range of specimen sizes with proportional dimensions is recommended. The dimension on which the proportionality is based is specimen thickness.

1.3 Requirements are set on specimen size and the number of replicate tests that are needed to establish acceptable characterization of K _Jc data populations.

1.4 The statistical effects of specimen size on K _Jc in the transition range are treated using weakest-link theory (1) applied to a three-parameter Weibull distribution of fracture toughness values. A limit on K _Jc values, relative to the specimen size, is specified to ensure high constraint conditions along the crack front at fracture. For some materials, particularly those with low strain hardening, this limit may not be sufficient to ensure that a single-parameter ( K _Jc ) adequately describes the crack-front deformation state (2) .

1.5 Statistical methods are employed to predict the transition toughness curve and specified tolerance bounds for 1T specimens of the material tested. The standard deviation of the data distribution is a function of Weibull slope and median K _Jc . The procedure for applying this information to the establishment of transition temperature shift determinations and the establishment of tolerance limits is prescribed.

1.6 The fracture toughness evaluation of nonuniform material is not amenable to the statistical analysis methods employed in this standard. Materials must have macroscopically uniform tensile and toughness properties. For example, multipass weldments can create heat-affected and brittle zones with localized properties that are quite different from either the bulk material or weld. Thick section steel also often exhibits some variation in properties near the surfaces. Metallography and initial screening may be necessary to verify the applicability of these and similarly graded materials. Data falling outside the 2 % or 98 % tolerance bounds may be indicative of a nonuniform material (see 9.3).

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

E4 Practices for Force Verification of Testing Machines

E8/E8M Test Methods for Tension Testing of Metallic Materials

E23 Test Methods for Notched Bar Impact Testing of Metallic Materials

E74 Practice of Calibration of Force-Measuring Instruments for Verifying the Force Indication of Testing Machines

E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods

E208 Test Method for Conducting Drop-Weight Test to Determine Nil-Ductility Transition Temperature of Ferritic Steels

E399 Test Method for Linear-Elastic Plane-Strain Fracture Toughness K Ic of Metallic Materials

E436 Test Method for Drop-Weight Tear Tests of Ferritic Steels

E561 Test Method for K-R Curve Determination

E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

E1820 Test Method for Measurement of Fracture Toughness

E1823 Terminology Relating to Fatigue and Fracture Testing

Keywords

temperature;

ICS Code

ICS Number Code 77.040.10 (Mechanical testing of metals)

DOI: 10.1520/E1921-02

ASTM International is a member of CrossRef.