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Description of ASTM-E1413 2019ASTM E1413-19Redline Standard: Standard Practice for Separation of Ignitable Liquid Residues from Fire Debris Samples by Dynamic Headspace Concentration onto an Adsorbent TubeASTM E1413Scope 1.1 This practice describes the procedure for separation of ignitable liquid residues from fire debris samples using dynamic headspace concentration onto an adsorbent tube, with subsequent solvent elution or thermal desorption. 1.2 Dynamic headspace concentration onto an adsorbent tube takes place from a closed, rigid sample container (typically a metal can), using a source of dry inert gas or a vacuum system. 1.3 Both positive and negative applied pressure systems for dynamic headspace concentration onto an adsorbent tube are illustrated and described. 1.4 This practice is suitable for preparing extracts from fire debris samples containing a range of volumes (µL to mL) of ignitable liquid residues, with sufficient recovery for subsequent qualitative analysis (1).2 1.5 Alternative headspace concentration methods are listed in Section 2 (see Practices E1388, E1412, E3189, and E2154). 1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.7 This standard cannot replace knowledge, skills, or abilities acquired through education, training, and experience (Practice E2917) and is to be used in conjunction with professional judgment by individuals with such discipline-specific knowledge, skills, and abilities. 1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. Keywords activated carbon; adsorbent tube; dynamic headspace concentration; elution; fire debris samples; forensic science; gas chromatography-mass spectrometry; ignitable liquid residues; Tenax TA; thermal desorption; ICS Code ICS Number Code 13.220.99 (Other standards related to fire protection) DOI: 10.1520/E1413-19 This book also exists in the following packages...Subscription InformationMADCAD.com ASTM Standards subscriptions are annual and access is unlimited concurrency based (number of people that can access the subscription at any given time) from single office location. For pricing on multiple office location ASTM Standards Subscriptions, please contact us at info@madcad.com or +1 800.798.9296.
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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