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  • ASTM
    D7442-22 Standard Practice for Sample Preparation of Fluid Catalytic Cracking Catalysts, Catalytic Materials, and Zeolites for Elemental Analysis by Inductively Coupled Plasma Optical Emission Spectroscopy (Redline)
    Edition: 2022
    $103.58
    Unlimited Users per year

Description of ASTM-D7442 2022

ASTM D7442-22

Redline Standard: Standard Practice for Sample Preparation of Fluid Catalytic Cracking Catalysts, Catalytic Materials, and Zeolites for Elemental Analysis by Inductively Coupled Plasma Optical Emission Spectroscopy




ASTM D7442

Scope

1.1 This practice covers uniform dissolution techniques for preparing samples of fluid catalytic cracking catalysts (FCC) and exchanged zeolitic materials for analysis by Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES). These techniques describe standardized approaches to well-known, widely used laboratory practices of sample preparation utilizing acid digestions and borate salt fusions. This practice is applicable to fresh and equilibrium FCC catalysts, catalytic materials used to manufacture catalyst, and exchanged zeolite materials.

1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Keywords

acid decomposition; atomic spectroscopy; catalyst; fluid catalytic cracking; fusion; hydrofluoric acid; inductively-coupled plasma emission spectroscopy; perchloric acid; zeolites;


ICS Code

ICS Number Code 71.040.50 (Physicochemical methods of analysis)


DOI: 10.1520/D7442-22

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