1. Scope

1.1 This sampling guide was developed for prebaked carbon anodes used in the production of aluminum, and details procedures for taking test samples from anode blocks. It covers equipment and procedures for obtaining samples from anode blocks in a manner that does not destroy the block or prevent its subsequent use as originally intended. However, the user must determine the subsequent use of the sampled anode blocks. Preferred locations for taking samples from single units of anodes are covered in this guide.

1.1.1 Information for sampling of shaped refractory products, in general, is given in ISO 5022. This standard details the statistical basis for sampling plans for acceptance testing of a consignment or lot. Anodes used in the production of aluminum have specific requirements for sampling and while the statistical basis for sampling given in ISO 5022 applies, further or modified requirements may, also, apply.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Note 1-The following ASTM standards are notes as sources of useful information: Test Methods C559, C611, C651, C747, C1025, C1039, and E1225.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

C559 Test Method for Bulk Density by Physical Measurements of Manufactured Carbon and Graphite Articles

C611 Test Method for Electrical Resistivity of Manufactured Carbon and Graphite Articles at Room Temperature

C651 Test Method for Flexural Strength of Manufactured Carbon and Graphite Articles Using Four-Point Loading at Room Temperature

C747 Test Method for Moduli of Elasticity and Fundamental Frequencies of Carbon and Graphite Materials by Sonic Resonance

C1025 Test Method for Modulus of Rupture in Bending of Electrode Graphite

C1039 Test Methods for Apparent Porosity, Apparent Specific Gravity, and Bulk Density of Graphite Electrodes

E1225 Test Method for Thermal Conductivity of Solids by Means of the Guarded-Comparative-Longitudinal Heat Flow Technique

ISO Standards

Keywords

anode; anthracite; carbon; core; graphite; prebaked; sample; sampling; test specimens;

ICS Code

ICS Number Code 77.020 (Production of metals)

DOI: 10.1520/D6353-98R03

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