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  • ASTM
    D6159-97(2012) Standard Test Method for Determination of Hydrocarbon Impurities in Ethylene by Gas Chromatography
    Edition: 2012
    $103.58
    Unlimited Users per year

Description of ASTM-D6159 2012

ASTM D6159 - 97(2012)

Standard Test Method for Determination of Hydrocarbon Impurities in Ethylene by Gas Chromatography

Active Standard ASTM D6159 | Developed by Subcommittee: D02.D0.02

Book of Standards Volume: 05.03




ASTM D6159

Significance and Use

4.1 High-purity ethylene is required as a feedstock for some manufacturing processes and the presence of trace amounts of certain hydrocarbon impurities can have deleterious effects. This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work.

4.2 This test method does not detect such impurities as H 2 O, CO, CO 2 , and alcohols that may be present in the sample. Hydrocarbons higher than n -decane cannot be analyzed by this test method, if present in the sample. Test Method D2504 addresses the analysis of noncondensable gases and Test Method D2505 addresses the analysis of CO 2 . Guide D5234 describes all potential impurities present in ethylene. These standards should be consulted when determining the total concentration of impurities in ethylene.

1. Scope

1.1 This test method covers the determination of methane, ethane, propane, propene, acetylene, iso -butane, propadiene, butane, trans-2-butene, butene-1, isobutene, cis-2-butene, methyl acetylene and 1,3-butadiene in high-purity ethylene. The purity of the ethylene can be calculated by subtracting the total percentage of all impurities from 100.00 %. Since this test method does not determine all possible impurities such as CO, CO 2 , H 2 O, alcohols, nitrogen oxides, and carbonyl sulfide, as well as hydrocarbons higher than decane, additional tests may be necessary to fully characterize the ethylene sample.

1.2 Data are reported in this test method as ppmV (parts per million by volume). This test method was evaluated in an interlaboratory cooperative study in the concentration range of 4 to 340 ppmV (2 to 204 mg/kg). The participants in the interlaboratory cooperative study reported the data in non-SI units. Wherever possible, SI units are included.

1.3 This standard dose not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D2504 Test Method for Noncondensable Gases in C2 and Lighter Hydrocarbon Products by Gas Chromatography

D2505 Test Method for Ethylene, Other Hydrocarbons, and Carbon Dioxide in High-Purity Ethylene by Gas Chromatography

D5234 Guide for Analysis of Ethylene Product


Keywords

ethylene; gas chromatography; hydrocarbon impurities;


ICS Code

ICS Number Code 71.040.50 (Physicochemical methods of analysis)


DOI: 10.1520/D6159-97R12

ASTM International is a member of CrossRef.

ASTM D6159

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ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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