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  • ASTM
    D6071-13 Standard Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atomic Absorption Spectroscopy
    Edition: 2013
    $103.58
    Unlimited Users per year

Description of ASTM-D6071 2013

ASTM D6071 - 13

Standard Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atomic Absorption Spectroscopy

Active Standard ASTM D6071 | Developed by Subcommittee: D19.03

Book of Standards Volume: 11.01




ASTM D6071

Significance and Use

5.1 Small quantities of sodium, 1 to 10 ?g/L, can be significant in high pressure boiler systems and in nuclear power systems. Steam condensate from such systems must have less than 10 ?g/L. In addition, condensate polishing system effluents should have less than 1 ?g/L. Graphite furnace atomic absorption spectroscopy (GFAAS) represents technique for determining low concentrations of sodium.

1. Scope

1.1 This test method covers the determination of trace sodium in high purity water. The method range of concentration is 1 to 40 ?g/L sodium. The analyst may extend the range once its applicability has been ascertained.

Note 1 It is necessary to perform replicate analysis and take an average to accurately determine values at the lower end of the stated range.

1.2 This test method is a graphite furnace atomic absorption spectrophotometric method for the determination of trace sodium impurities in ultra high purity water.

1.3 This test method has been used successfully with a high purity water matrix. 2 It is the responsibility of the analyst to determine the suitability of the test method for other matrices.

1.4 The values stated in SI units are to be regarded as standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D1066 Practice for Sampling Steam

D1129 Terminology Relating to Water

D1192 Guide for Equipment for Sampling Water and Steam in Closed Conduits

D1193 Specification for Reagent Water

D2777 Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water

D3370 Practices for Sampling Water from Closed Conduits

D3919 Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry

D4453 Practice for Handling of High Purity Water Samples

D5810 Guide for Spiking into Aqueous Samples

D5847 Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis


Keywords

graphite furnace atomic absorption spectroscopy (GFAAS); high purity water; sodium ;


ICS Code

ICS Number Code 71.040.50 (Physicochemical methods of analysis)


DOI: 10.1520/D6071-13

ASTM International is a member of CrossRef.

ASTM D6071

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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