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  • ASTM
    D5808-23 Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry (Redline)
    Edition: 2023
    $103.58
    Unlimited Users per year

Description of ASTM-D5808 2023

ASTM D5808-23

Redline Standard: Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry




ASTM D5808

Scope

1.1 This test method covers the determination of organic chloride in aromatic hydrocarbons, their derivatives, and related chemicals.

1.2 This test method is applicable to samples with chloride concentrations to 25 mg/kg. The limit of detection (LOD) is 0.2 mg/kg and the limit of quantitation (LOQ) is 0.7 mg/kg. With careful analytical technique or the measurement of replicates, or both, this method can be used to successfully analyze concentrations below the LOD.

Note 1: The maximum is the highest concentration from the interlaboratory study and the LOD and LOQ were calculated from Performance Testing Program (PTP) data. See Table 1.

1.3 This test method is preferred over Test Method D5194 for products, such as styrene, that are polymerized by the sodium biphenyl reagent.

1.4 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.5 Organic chloride values of samples containing inorganic chlorides will be biased high due to partial recovery of inorganic species during combustion. Interference from inorganic species can be reduced by water washing the sample before analysis. This does not apply to water soluble samples.

1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 7.3 and Section 9.

1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Keywords

density; electrolysis; electrolyte; microcoulometry; potential; pyrolysis; recovery factor; relative density; titration; total chloride; volatilization;


ICS Code

ICS Number Code 71.040.40 (Chemical analysis)


DOI: 10.1520/D5808-23

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ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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