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Description of ASTM-D4821 2019ASTM D4821-19Historical Standard: Standard Guide for Carbon Black—Validation of Test Method Precision and BiasASTM D4821Scope 1.1 This guide covers procedures for using the ASTM Standard Reference Blacks2 (SRBs) and the HT and INR Iodine Number Standards to continuously monitor the precision of those carbon black test methods for which reference values have been established. It also offers guidelines for troubleshooting various test methods. 1.2 This guide defines the environmental conditions that are required for laboratories that perform carbon black testing activities for those test methods under D24’s jurisdiction. 1.3 This guide establishes procedures for the use of x-charts to continuously monitor those tests listed in Section 2 for within-lab precision (repeatability) and between-lab accuracy (reproducibility). 1.4 This guide provides a statistical procedure for improving test reproducibility when a laboratory cannot physically calibrate its apparatus to obtain the reference values of the ASTM reference blacks, within the ranges given in this guide. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. Keywords accuracy; ASTM reference blacks; carbon black; continuously monitoring testing; laboratory environmental conditions; normalization; precision; regression; repeatability; reproducibility; statistical x-charts; ICS Code ICS Number Code 83.040.20 (Rubber compounding ingredients) DOI: 10.1520/D4821-19 The following editions for this book are also available...
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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