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Description of ASTM-D4503 1998ASTM D4503-86-Reapproved1998Historical Standard: Standard Practice for Dissolution of Solid Waste by Lithium Metaborate FusionASTM D4503Scope 1.1 This practice covers the drying, ashing, and solubilization of solid waste using a lithium metaborate (LiBO2) fusion for the subsequent determination of inorganic constituents by argon plasma emission spectroscopy or atomic absorption spectroscopy. 1.2 The following elements may be solubilized by this practice: aluminum chromium silicon barium iron titanium cadmium magnesium vanadium calcium manganese zinc copper nickel1.3 This practice has been used successfully with a bauxite ore and a neutralized metal treatment sludge. The practice may be applicable to other elements not listed above. Some metals, such as cadmium and zinc, may volatilize from some samples during the drying, ashing, or fusion steps. The analyst is responsible for determining whether the practice is applicable to the solid waste being tested. 1.4 This practice is intended for the solubilization of nonvolatile inorganic constituents in solid waste. The LiBO2 fusion is appropriate for a silicate matrix or acid resistant samples. 1.5 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 7. Keywords Aluminum; Aluminum alloys; Ashing; Barium; Bauxite ore; Cadmium; Calcium; Chromium; Copper; Drying; Fusion; Inorganic compounds; Iron; Iron alloys; Lithium metaborate fusion; Magnesium; Manganese; Municipal solid waste (MSW); Neutralized metal treatment sludge; Nickel; Resource recovery; Silicon; Sludge; Solubilization; Spectroscopy-argon plasma; Titanium; Vanadium; Zinc; dissolution of solid waste, by lithium metaborate fusion, practice ICS Code ICS Number Code 13.030.10 (Solid wastes) DOI: 10.1520/D4503-86R98 This book also exists in the following packages...Subscription InformationMADCAD.com ASTM Standards subscriptions are annual and access is unlimited concurrency based (number of people that can access the subscription at any given time) from single office location. For pricing on multiple office location ASTM Standards Subscriptions, please contact us at info@madcad.com or +1 800.798.9296.
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