1. Scope

1.1 This test method covers the determination of the purity of isopropylbenzene (cumene) by gas chromatography.

1.2 This test method has been found applicable to the measurement of impurities such as nonaromatic hydrocarbons, benzene, ethylbenzene, t -butylbenzene, n -propylbenzene, alpha-methylstyrene, sec-butylbenzene, and diisopropylbenzene, which are common to the manufacturing process of isopropylbenzene. Limit of detection for these impurities is 10 mg/kg (see 5.1).

1.3 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off 'to the nearest unit' in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D3437 Practice for Sampling and Handling Liquid Cyclic Products

D6809 Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E260 Practice for Packed Column Gas Chromatography

E355 Practice for Gas Chromatography Terms and Relationships

E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

E1510 Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs

Keywords

alpha methylstyrene; analysis by gas chromatography; benzene; butylbenzene; cumene; ethylbenzene; isopropylbenzene; nonaromatic hydrocarbons; propylbenzene;

ICS Code

ICS Number Code 71.080.10 (Aliphatic hydrocarbons)

DOI: 10.1520/D3760-02

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