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Description of ASTM-D1552 2023ASTM D1552-23Active Standard: Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)ASTM D1552Scope 1.1 This test method covers procedures for the determination of total sulfur in petroleum products including lubricating oils containing additives, and in additive concentrates. This test method is applicable to samples boiling above 177 °C (350 °F). Other sulfur concentrations outside of those listed in 1.1.1 and 1.1.2 may be analyzed, but the precision stated may or may not apply. These procedures use IR detection or TCD following combustion in a furnace. 1.1.1 Procedure A, IR Detection: 1.1.1.1 This procedure is applicable to samples containing a mass fraction of sulfur between 0.22 % and 24.2 %. 1.1.1.2 Petroleum coke containing a mass fraction of sulfur between 2.53 % to 3.79 % sulfur may be analyzed. 1.1.2 Procedure B, TCD Detection: 1.1.2.1 This procedure is applicable to samples containing a mass fraction of sulfur between 0.071 % and 25.8 %. 1.1.2.2 Petroleum coke containing a mass fraction of sulfur between 0.19 % to 6.38 % sulfur may be analyzed. 1.2 Petroleum coke containing a mass fraction of sulfur between 2.53 % to 3.79 % sulfur may be analyzed. Other sulfur concentrations may be analyzed, but the precision stated may or may not apply. Note 1: The D1552 – 08 (2014) version of this standard contained two other procedures using iodate titrations. Since these procedures are no longer being used in the industry laboratories based on a survey of D02.SC 3 laboratories conducted in September 2014, they are being deleted. For earlier information on the deleted procedures, D1552 – 08 (2014) may be perused. 1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. Keywords coke; combustion; furnace; high temperature; IR detection; petroleum; resistance furnace; sulfur; thermal conductivity detection; ICS Code ICS Number Code 75.080 (Petroleum products in general) DOI: 10.1520/D1552-23 The following editions for this book are also available...
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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